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Lc Ms Articles & Analysis

19 articles found

Advancing Research Through Accurate Fatty Acids Quantification in Agricultural Science

Advancing Research Through Accurate Fatty Acids Quantification in Agricultural Science

GC-MS fatty acid profiling often starts with the transesterification of lipids into fatty acid methyl esters (FAMEs), followed by chromatographic separation. ...

ByLifeasible


Pesticide Registration GLP 5 Batch Analysis

Pesticide Registration GLP 5 Batch Analysis

Impurities can be identified and their composition and structure can be ascertained by the use of sophisticated analytical techniques such as GC-MS, LC-MS-MS, and NMR. Step 3: Determination of Analytical Reference Standards To guarantee accurate results, these analytical reference standards are employed as benchmarks throughout ...

ByProtheragen-ING


Beyond Chemistry: Discover the Power of Pheromone Activity Screening

Beyond Chemistry: Discover the Power of Pheromone Activity Screening

Pheromone activity screening service is provided with advanced analytical techniques including Gas Chromatography-Mass Spectrometry (GC-MS), Liquid Chromatography-Mass Spectrometry (LC-MS), and Nuclear Magnetic Resonance (NMR) Spectroscopy to identify and isolate the components of pheromone blends. ...

ByAlfa Chemistry


How to Use Labels in Your Growing Cannabis Business

How to Use Labels in Your Growing Cannabis Business

This is usually performed by taking a sample of cannabis extract and analyzing its components, including cannabinoids and terpenes, via high-performance liquid chromatography (HPLC), liquid chromatography with mass spectrometry (LC-MS), gas chromatography (GC), or thin-layer chromatography (TLC). ...

ByGA International Inc.


What are the most common forms of Cannabis testing?

What are the most common forms of Cannabis testing?

Some of the instruments which can be used for terpene testing include: In addition to Peak Scientiifc's Precision series of gas geneartors for gas chromatography, the Solaris XE 35 nitrogen generator could also be used for terpene testing with LC-MS instruments. To discover Peak's full range of gas generators for LC-MS please ...

ByPEAK Scientific Instruments Ltd


Neonicotinoids

Neonicotinoids

Our certified reference materials are produced and analyzed under double accreditation ISO/IEC 17025 and ISO 17034 to give you accuracy assurance. Analytical Method LC/MS/MS Analysis of Neonicotinoid Pesticides in Dandelion Blossoms on Ascentis® Express C18 after Dispersive SPE (QuEChERS) Read More ...

ByMerck KGaA, Darmstadt, Germany


Quality Control in the Growing Cannabis Market

Quality Control in the Growing Cannabis Market

This analysis is usually carried out using LC-MS (Liquid Chromatography Mass Spectrometry) or GC (Gas Chromatography). LC-MS and GC require a flow of inert gas such as hydrogen or nitrogen, both of which can be easily supplied via a gas generator. ...

ByPEAK Scientific Instruments Ltd


An automated extraction solution for the determination of Melamine and Cyanuric Acid in Milk Based Products

An automated extraction solution for the determination of Melamine and Cyanuric Acid in Milk Based Products

In this study, the performance and versatility of the AutoMate-Q40, workstation platform, was evaluated for the extraction of Melamine and Cyanuric Acid in milk based products. A Liquid Chromatography (LC) coupled to a Triple-Quadrupole Mass Spectrometer (LC-MS/MS) was employed for the detection of these adulterants. ...

ByTeledyne Tekmar


Soil organic matter content effects on dermal pesticide bioconcentration in American toads (Bufo americanus)

Soil organic matter content effects on dermal pesticide bioconcentration in American toads (Bufo americanus)

Whole body tissue homogenates and soils were extracted and analyzed using LC‐MS to determine pesticide tissue and soil concentration, as well as bioconcentration factor in toads. ...

ByJohn Wiley & Sons, Ltd.


Field degradation of aminopyralid and clopyralid and microbial community response to application in Alaskan soils

Field degradation of aminopyralid and clopyralid and microbial community response to application in Alaskan soils

Quantification was performed via LC/MS‐MS and microbial diversity assessed via next‐generation sequencing of bacterial 16S rRNA genes. ...

ByJohn Wiley & Sons, Ltd.


An Automated Extraction Solution for Imidazolinone Herbicides

An Automated Extraction Solution for Imidazolinone Herbicides

In this study, the performance and versatility of the AutoMate-Q40, QuEChERS workflow solution, was evaluated for the extraction of Imidazolinone herbicides. A Liquid Chromatograph (LC) coupled to a Triple-Quadrupole Mass Spectrometer (LC-MS/MS) was employed for the detection of these herbicides in agricultural commodities. ...

ByTeledyne Tekmar


Mowing mitigates bioactivity of neonicotinoid insecticides in nectar of flowering lawn weeds and turfgrass guttation

Mowing mitigates bioactivity of neonicotinoid insecticides in nectar of flowering lawn weeds and turfgrass guttation

We applied imidacloprid or clothianidin to turf with white clover, followed by irrigation, and used LC‐MS/ MS to analyze residues in clover blooms that were directly sprayed during application or that formed after the first mowing. ...

ByJohn Wiley & Sons, Ltd.


Evaluation of EN15662:2008 - Determination of Pesticide Residue in Food of Plant Origin, by an Automated QuEChERS Solution

Evaluation of EN15662:2008 - Determination of Pesticide Residue in Food of Plant Origin, by an Automated QuEChERS Solution

The analyses typically involve use of multi-residue methods (both GC-MS and LC-MS) to test for over 500 pesticide residues. Due to its ease of use and proven robustness, the QuEChERS extraction has become the method of choice for pesticides multi-residue analyses in a wide range of matrices. This study used laboratory spiked samples and samples ...

ByTeledyne Tekmar


Determination of Highly Polar Pesticide Residues in Food of Plant Origin, by an Automated QuPPe Solution

Determination of Highly Polar Pesticide Residues in Food of Plant Origin, by an Automated QuPPe Solution

In 2008 at EPRW in Berlin the “Quick Method for Analysis of Residues of numerous Highly Polar Pesticides in Food of Plant Origin involving Simultaneous Extraction with Methanol and LC-MS/MS Determination” (QuPPe Method) was presented. The aim of this project is to evaluate the performance and versatility of the AutoMate-Q40 for the ...

ByTeledyne Tekmar


COMPARATIVE PHARMACEUTICAL METABOLISM BY RAINBOW TROUT (ONCORHYNCHUS MYKISS) LIVER S9 FRACTIONS

COMPARATIVE PHARMACEUTICAL METABOLISM BY RAINBOW TROUT (ONCORHYNCHUS MYKISS) LIVER S9 FRACTIONS

An isotope dilution liquid chromatography tandem mass spectrometry (LC‐MS/MS) method was employed for quantitation of parent chemical concentrations. ...

ByJohn Wiley & Sons, Ltd.


LC/MS/MS Analysis of Mycotoxins

LC/MS/MS Analysis of Mycotoxins

Food safety is ensured by testing for the presence of mycotoxins by methods such as LC-MS-MS. In addition to mycotoxins, many other known and unknown chemicals threaten the food supply, however their presence might be missed by LC-MS-MS methods which rely exclusively on MRM settings for ...

ByShimadzu Scientific Instruments Inc


Free and Conjugated Estrogen Exports in Surface-Runoff from Poultry Litter–Amended Soil

Free and Conjugated Estrogen Exports in Surface-Runoff from Poultry Litter–Amended Soil

Estrogen concentrations were screened using enzyme-linked immunosorbent assay (ELISA), followed by quantification using liquid chromatography with tandem mass spectrometry (LC/MS/MS). Concentrations of estrogens from ELISA were much higher than the LC/MS/MS values, indicating cross-reactivity ...

ByThe American Society of Agronomy (ASA)


Application of a GPC-LC-MS/MS method for the determination of 31 mycotoxins in edible oils

Application of a GPC-LC-MS/MS method for the determination of 31 mycotoxins in edible oils

Gel Permeation Chromatography (GPC) is widely used for sample clean up in mycotoxin analysis. The most commonly described methods use GPC columns packed with SX-3 BioBeads suitable for cleaning Zearalenone, Aflatoxins and Trichothesenes from edible oils and fatty matrices. Separation of Fumonisins from the oil fraction are inadequate with this column. The new GPC column designed by LCTech shows ...

ByPickering Laboratories, Inc.


Mycotoxins: Emergent Health Issue in IAQ

Mycotoxins: Emergent Health Issue in IAQ

These techniques can provide the IAQ professional with useful data for only a fraction of the cost than that of more sophisticated techniques that use liquid chromatography with mass spectrometry (LC/MS). LC/MS is useful for very low level detection and identification of certain mycotoxins and metabolites where no ...

ByEMSL Analytical, Inc.

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